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HAND BOOK OF FLAVOURS TECHNOLOGY

FLAVOUR ANALYSIS

Sample Preparation
Isolation of Food Flavours
Headspace Methods
Direct Injection
Headspace Concentration
Cryogenic Trapping
Adsorbent Trapping
Isolation of Flavours by Distillation Methods
Isolation of Flavours by Solvent Extraction
Equipment and Procedures
Solvent Selection
Solvent Impurities
Solvent Extraction of Fatty Foods
Isolation of Individual Classes of Volatile Flavours
Sulfur Compounds
Acids
Alcohols
Carbonyls
Evaporation
Freeze Concentration
Adsorption
Flavour Analysis by Direct Injection
Gas Chromatography
Fractionation of Flavour Isolates
Gas Chromatography of Flavour Concentrates
Capillary Column GC
Chiral Gas Chromatography
GC Detectors
Quantification
High Pressure Liquid Chromatography
Identification of Volatile Flavours
Summary

CHEMISTRY OF FLAVOURS

Introduction
Flavour Classification
Flavour Formation in Plants
Biogenesis of Fruits Aroma
Flavours from Fatty Acid Metabolism
Flavours Formed from Carbohydrate Metabolism
Flavour Formation in Vegetables
Flavour Formation from Cysteine Sulfoxide Derivatives
Flavour formation from Gluconsinolates
Additional Pathways for Vegetable Flavour Formation
Location of Flavour in Plant
Influence of Genetics, Nutrition Environment, Maturity and Storage on Flavour
Conclusions
Chemistry of Essential Oils
Terpenes
Oxygenated erpenoid Compounds
Benzenoid Compounds
Compounds Containing Nitrogen and Sulfur
Nitrogen Compounds
Sulfur compounds
Sulfur Containing Oils
White Mustard
Black (Brown) Mustard
Fruit Flavours
Aromatic Components
Fruit Sugars and Acids
Sugars
Monosaccharides
Disaccharides
Trisaccharides
Nonsugars (Polysaccharides)
Flavour of Dairy Products
Milk
Cheese
Flavour Development
Fatty Acids
Carbonyls
Sulfur Compounds
Amino Acids and Peptides
Flavour Balance
Roquefort (Blue) Cheese Flavour
Flavour Development
Fermentation
Fungi
Black Tea Aroma
Flavour Formation During Thermal Processing
Nonenzymatic Browing
General Overview of Maillard Browing
Factors influencing Browning Rate
Temperature
pH
Water Activity
Influence of Fat
Summary
Formation of Flavour Comounds
Flavours from Lipids
Hydrolytic Reactions
Oxidation
Pyrolysis Reactions
Effect of Frying Condition on Flavour
Mechanisms of Flavour Formation
Lactones
Seafood Flaovurs
Caramelization
Flavours Formed Via Fermentation
Esters
Acids
Carbonyis
Alcohols
Terpenes
Lactones
Pyrazines
Conclusions

OFF FLAVOURS IN FOODS

Environmental Contamination
Waterborne Sources
Off Flavours Due to In-Plant Water Contamination
Tainting of Aquatic Animals by Contaminated Water
Disinfectants, Pesticides and Detergents
Packaging Sources
Food Contamination
Flavour Scalping
Packaging Catalyzed Off Flavours
Oxygen/Wate Vapour Transmission
Off Flavours Due to Genetics or Diet
Off Flavours Due to Chemical Changes in the Food
Nonenzymatic Browning
Photo Induced Off Flavours
Milk
Beer and Champagne
Enzymatic Flavour Changes
Lipoxygenase
Lipase
Proteolytic Enzymes
Microbial Off Flavours
Summary

MANUFACTURING PROCESSES OF FLAVOURS

Introduction
The Thermally Processed Flavours (Meat and Savory Flavours)
Yeast and Autolyzed Yeast Extracts
Basic Process Flavourings
Complex Process Flavourings
The Final Flavour
Enzyme Modification and Fermentation The Dairy Flavours
Milk and Cream Flavours
Cultured Dairy Flavours
Butter Flavour
Cheese Flavours
Creation of Dairy Flavours
Regulatory Issues
Appendix 4.1 IOFI Guidelines for the Production and Labeling of Process Flavours
Introduction
Scope
Definition
Basic Standards of Good Manufacturing Practice
Production of Process Flavourings
Raw Materials for Process Flavourings
Preparation of Process Flavourings
Appendix Table-A4.1
Labeling

PLANT MATERIALS USED IN FLAVOURINGS

172.510 Natural Flavouring Substances and Natural Substances and Natural Substances Used in Conjunction with Flavours
182.10 Spices and Other Natural Seasonings and Flavourings
182.20 Essential Oils, Oleoresins (Solvent-Free), and Natural Extractives (Including Distillates)
182.40 Natural Extractives (Solvent Free) Used in Conjunction with Spices, Seasonings, and Flavourings

PRINCIPAL ESSENTIAL OILS USED IN FLAVOURINGS

APPLICATION OF FLAVOURINGS IN FOOD PROCESSING

Flavours in Foods
Achieving Flavour Balance
Consumer Acceptance
Flavour Defects
Flavour Intensification
Flavour Suppression
Criteria for Application of Flavourings
Acceptability to the Consumer
Legal Acceptability
Nature of Product as Sold and as Consumed
Processing Conditions
Available Flavourings
Processing Parameters
Temperature and Time
Open or Closed System
The Mixing Sequence
pH
Pressure
Contact with Air
specific Flavouring Applications
Meat Products
Baked Goods and Bakey Products
Snack Foods
Sugar and Chocolate Confectionery
Pickles and Sauces
soups
Ice Cream and Frozen Goods
Soft Drinks
Conclusion

QUALITY CONTROL

Analytical Tests
Overview of Physicohemical Tests
Natural Plant Materials
General Tests
Tests of Limited Application
Additional Specific Tests
Essential Oils
General Tests
Tests of Limited Application
Instrumental Tests
Specific Test for Constituents
Tests Specific for Citrus Oils
Specific Tests and Producedures
Oleoresins
General Tests
Specific Tests
Plated or Dispersed Spices
General Tests
Tests of Limited Application
synthetic Chemicals
General Tests Liquids
General Tests Solids
Specific Tests for Chemical Identity and Purity Instrumental Methods
Flavourings
General Tests Liquid Flavourings
General Tests Emulsions
General Tests Encapsulated Dry Flavourings
Vanilla Extract
Fruit Based Products
General Tests
Special Tests
Specific Gravity
Refractive Index
Optical Rotation
Alcohol Content
Residual Solvent
Practicle Size of Emulsions
Volatile Oil
Surface Oil
Moisture Content
Gas Chromatography
Microbiological Analysis
Sensory Analysis

NON-ALCOHOLIC FLAVOURS

Compounding
Plant Economics of Non-Alcoholic Flavours
Plant & Machinery
Other Fixed Assets
Fixed Capital
Raw Materials
Total Working Capital/Month
Total Capital Investment
Turn Over/Annum

FLAVOURS FRUIT (WHISKEY, VODKA, GRAPE, BUTTER SCOTCH AND RUM)

Artificial Flavourings
Manufacturing Process
For Rum Flavour
Process Flow Diagram for Rum Flavour
Plant Economics of Fruit Flavours
Plant and Machinery
Other Fixed Assets
Fixed Capital
Raw Materials
For Rum Flavour
For Whiskey Flavour
For Grape Flavour
For Butter Scotch Flavour
Total Woring Capital/Month
Total Capital Investment
Turn Over/Annum

TERPENELESS MENTHOL CRYSTALS

Manufacturing Process Fractional Distillation of D.M.O. for Removal of Terpene
Extraction of Menthol
Crystallization
Separation of the Menthol Crystals from the Dementholized Oil
Drying of Menthol Crystals
Yield of Menthol & Dementholized Mint Oil
Plant Economics of Terpeneless Menthol Crystals
Plant & Machinery
Other Fixed Assets
Fixed Capital
Raw Materials
Total Working Capital/Month
Total Capital Investment
Turn Over/Annum

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